Structure, Microstructure, and Properties of Modified Ceramics (Na,Sr)0.5Bi0.5TiO3

G. M. Kaleva; Калева Г. М.; E. D. Politova; Политова Е. Д.; A. V. Mosunov; Мосунов А. В.; S. Yu. Stefanovich; Стефанович С. Ю.; T. S. Ilina; Ильина Т. С.; D. A. Kiselev; Киселев Д. А.; N. V. Sadovskaya; Садовская Н. В.

doi:10.31857/S002347612360043X

Structure, Microstructure, and Properties of Modified Ceramics (Na,Sr)0.5Bi0.5TiO3

Authors: Kaleva G.M.¹, Politova E.D.¹, Mosunov A.V.², Stefanovich S.Y.², Ilina T.S.³, Kiselev D.A.³, Sadovskaya N.V.⁴
Affiliations:
1. Semenov Institute of Chemical Physics, Russian Academy of Sciences, 119991, Moscow, Russia
2. Moscow State University, 119991, Moscow, Russia
3. National University of Science and Technology MISiS, 119049, Moscow, Russia
4. Shubnikov Institute of Crystallography, Federal Scientific Research Centre “Crystallography and Photonics,” Russian Academy of Sciences, 119333, Moscow, Russia
Issue: Vol 68, No 5 (2023)
Pages: 817-825
Section: НАНОМАТЕРИАЛЫ, КЕРАМИКА
URL: https://rjmseer.com/0023-4761/article/view/673368
DOI: https://doi.org/10.31857/S002347612360043X
EDN: https://elibrary.ru/EDKICO
ID: 673368

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Abstract

Single-phase ceramic samples of new compositions (Na1 – хSrх)0.5Bi0.5TiO3 (x = 0–0.5), including those modified by additives of SiO2 and ZnO oxides, have been obtained by solid-phase synthesis. The crystal structure and microstructure of these samples, as well as their dielectric, nonlinear optical, and local piezoelectric properties, have been studied. The formation of a perovskite-type phase with a pseudocubic unit cell in all synthesized samples and an increase in the cell volume as a result of partial substitution of perovskite structure cations are established. A decrease in the temperature of ferroelectric phase transitions (confirmed by the methods of dielectric spectroscopy and laser second-harmonic generation) to the tetragonal paraelectric phase is revealed. Remanent piezoelectric hysteresis loops are obtained for the synthesized samples in the polarization switching mode; this result confirms the occurrence of ferroelectric polarization switching.

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