Sodium Chromium Arsenate Phosphates: Preparation, Structure, and Thermal Properties

E. A. Pyaterikov; Пятериков Е. А.; V. I. Pet’kov; Петьков В. И.; D. G. Fukina; Фукина Д. Г.; E. Yu. Borovikova; Боровикова Е. Ю.

doi:10.31857/S0044457X23600482

Sodium Chromium Arsenate Phosphates: Preparation, Structure, and Thermal Properties

Authors: Pyaterikov E.A.¹, Pet’kov V.I.¹, Fukina D.G.¹, Borovikova E.Y.²
Affiliations:
1. Nizhny Novgorod State University
2. Kola Scientific Center, Russian Academy of Sciences
Issue: Vol 68, No 10 (2023)
Pages: 1388-1397
Section: СИНТЕЗ И СВОЙСТВА НЕОРГАНИЧЕСКИХ СОЕДИНЕНИЙ
URL: https://rjmseer.com/0044-457X/article/view/666168
DOI: https://doi.org/10.31857/S0044457X23600482
EDN: https://elibrary.ru/TRMMFF
ID: 666168

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Abstract

Arsenate phosphates
(1.75 ≤ x ≤ 3.0) were prepared by coprecipitation. Their unit cell parameter was a linear function of composition: a (Å) = 0.0967x + 11.873. The Na3Cr2(AsO4)2PO4 crystal structure was refined by the Rietveld method; the coordinates of basal atoms and bond lengths were calculated. A garnet solid solution crystallizes at 600–650°C; transition to a high−temperature rhombohedral structure occurred at 994–1044°C. The thermal expansion of the low-temperature phase having a garnet structure was studied in the range from –130 to 200°C. The solid solution samples expanded isotropically and had small thermal expansion.

Keywords

garnet, arsenate phosphates, solid solution, thermal expansion

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