Optical ceramics obtained by hot pressing of CVD-ZnSe powder

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Resumo

The influence of mechanical grinding conditions of high-purity CVD zinc selenide (ZnSe) powders on their particle size distribution, their sintering process, and the transparency of optical ceramics has been studied. Powders with an optimal granulometric composition were obtained, having an average particle size of 0.3 μm with a maximum of not more than 1 μm. These parameters were achieved by grinding the powders in a planetary ball mill for 20 hours at a grinding bowl rotation speed of 150 rpm. ZnSe optical ceramics are fabricated by a combination of hot pressing and subsequent hot isostatic pressing of CVD powders. The maximum transmission for 2 mm thick samples was 69% (close to theoretically achievable) at a wavelength of 14 μm. The combination of characteristics of CVD ZnSe powders subjected to additional grinding shows their promise for use in optical ceramic technology.

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Sobre autores

S. Balabanov

G.G. Devyatykh Institute of Chemistry of High-Purity Substances of RAS

Autor responsável pela correspondência
Email: timofeeva@ihps-nnov.ru
Rússia, Nizhny Novgorod, 603137

N. Timofeeva

G.G. Devyatykh Institute of Chemistry of High-Purity Substances of RAS

Email: timofeeva@ihps-nnov.ru
Rússia, Nizhny Novgorod, 603137

T. Evstropov

G.G. Devyatykh Institute of Chemistry of High-Purity Substances of RAS

Email: timofeeva@ihps-nnov.ru
Rússia, Nizhny Novgorod, 603137

D. Kosyanov

Far Eastern Federal University

Email: timofeeva@ihps-nnov.ru
Rússia, Vladivostok, 690922

A. Naumova

G.G. Devyatykh Institute of Chemistry of High-Purity Substances of RAS

Email: timofeeva@ihps-nnov.ru
Rússia, Nizhny Novgorod, 603137

S. Filofeev

G.G. Devyatykh Institute of Chemistry of High-Purity Substances of RAS

Email: timofeeva@ihps-nnov.ru
Rússia, Nizhny Novgorod, 603137

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2. Fig. 1. Effect of milling time (0, 6, 12, 20 and 40 h) on the integral curves of particle size distribution volume curves for CVD ZnSe powders.

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3. Fig. 2. Effect of milling time on specific surface area SBET and equivalent particle diameter dBET of CVD ZnSe powders.

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4. Fig. 3. Microphotographs of CVD powders of ZnSe after milling for 2 (a) and 60 h (b).

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5. Fig. 4. Appearance of ZnSe ceramic samples from CVD powders with different milling times.

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6. Fig. 5. Transmission spectra of ZnSe ceramics obtained from CVD powders with milling times of 0, 2, 6, 12, and 20 h.

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7. Fig. 6. Photographs of pores in the volume of ZnSe 2 (a) and 20 (b) ceramics.

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8. Fig. 7. Histograms of grain size distribution for ZnSe ceramics: samples 0 (a), 12 (b), 20 (c).

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9. Fig. 8. Photographs of microstructures of ZnSe ceramics: samples 6 (a) and 20 (b).

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