Layered composite material of niobium–ceramic

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Abstract

Layered composite materials based on niobium and cermet were produced via self-propagating high-temperature synthesis of pre-structured samples using metal foils (Ti, Nb, Ta, Ni) and reaction tapes (Ti + 1.7B) and (5Ti + 3Si). Reaction tapes for synthesis were produced by rolling process of powder mixtures. The microstructure, elemental and phase compositions of the synthesized multilayer composite materials were studied by scanning electron microscopy and X-ray phase analysis. Particular attention was paid to the formation of intermediate layers and surface modification occurring during combustion. The strength characteristics of synthesized materials were determined according to the three-point loading scheme at temperatures of 1100°C. The analysis of obtained materials showed that joining in the combustion mode of metal foils and reaction tapes is provided due to reaction diffusion, mutual impregnation and chemical reactions occurring in the reaction tapes and on the surface of metal foils. The formation of thin intermediate layers in the form of cermet and eutectic solutions provides the synthesized multilayer materials with good strength properties up to 87 MPa at 1100°C. These results are of interest for the development of structural materials operating under extreme conditions.

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About the authors

O. K. Kamynina

Osipyan Institute of Solid State Physics RAS

Author for correspondence.
Email: kamynolya@gmail.com
Russian Federation, 142432, Chernogolovka

S. G. Vadchenko

Merzhanov Institute of Structural Macrokinetics and Materials Science RAS

Email: kamynolya@gmail.com
Russian Federation, 142432, Chernogolovka

I. D. Kovalev

Merzhanov Institute of Structural Macrokinetics and Materials Science RAS

Email: kamynolya@gmail.com
Russian Federation, 142432, Chernogolovka

D. V. Prokhorov

Osipyan Institute of Solid State Physics RAS

Email: kamynolya@gmail.com
Russian Federation, 142432, Chernogolovka

D. E. Andreev

Merzhanov Institute of Structural Macrokinetics and Materials Science RAS

Email: kamynolya@gmail.com
Russian Federation, 142432, Chernogolovka

A. N. Nekrasov

Institute of Experimental Mineralogy RAS

Email: kamynolya@gmail.com
Russian Federation, 142432, Chernogolovka

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2. Fig. 1. Initial sample structured from refractory metal foils and reaction tapes.

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3. Fig. 2. Distribution map of elements of the synthesized sample.

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4. Fig. 3. Diffraction pattern of the synthesized sample.

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5. Fig. 4. Morphology of the sample region corresponding to layers L1–L9 (Table 2).

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6. Fig. 5. Morphology of the sample region corresponding to layers L9–L17 (Table 2).

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7. Fig. 6. Fracture diagram at 1100°C (a) and morphology of the sample after three-point bending tests (b).

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